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§177.1990 偏二氯乙?丙烯酸甲酯共聚物(Vinylidene chloride/methyl acrylate copolymers)

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放大字体缩小字体2011-10-12 07:58:15 来源9a href="http://www.law.cornell.edu/cfr/text/21/177/1990" target="_blank" rel="nofollow">GPO浏览次数9span id="hits">2616
核心提示:偏二氯乙烯/丙烯酸甲酯共聚物,由偏二氯乙烯和丙烯酸甲酯经共聚作用而制得的基本共聚物组成,来自丙烯酸甲酯的量不超过共聚物量?5%。偏二氯乙烯/丙烯酸甲酯共聚物中可根据需要而含有某些辅料。这些辅料包?70?79部分中规定的物质、一般公认为在食品中安全的物质,在已公布的法规中允许使用的物质。本节还规定了偏二氯乙烯/丙烯酸甲酯共聚物的质量指标和分析方法、/div>
发布单位
FDA
FDA
发布文号 54 FR 24898
发布日期 1989-06-11 生效日期 暂无
有效性状?/th> 废止日期 暂无
备注 偏二氯乙?丙烯酸甲酯共聚物,由偏二氯乙烯和丙烯酸甲酯经共聚作用而制得的基本共聚物组成,来自丙烯酸甲酯的量不超过共聚物量?5%。偏二氯乙烯/丙烯酸甲酯共聚物中可根据需要而含有某些辅料。这些辅料包?70?79部分中规定的物质、一般公认为在食品中安全的物质,在已公布的法规中允许使用的物质。本节还规定了偏二氯乙烯/丙烯酸甲酯共聚物的质量指标和分析方法、/td>

177.1990 Vinylidene chloride/methyl acrylate copolymers


   The vinylidene chloride/methyl acrylate copolymers (CAS Reg. No. 25038-72-6 identified in paragraph (a of this section may be safely used as an article or as a component of an article intended for use in contact with food subject to the provisions of this section.

  (a Identity. For the purposes of this section vinylidene chloride/methyl acrylate copolymers consist of basic copolymers produced by the copolymerization of vinylidene chloride and methyl acrylate such that the copolymers contain not more than 15 weight-percent of polymer units derived from methyl acrylate.

  (b Optional adjuvant substances. The basic vinylidene chloride/methyl acrylate copolymers identified in paragraph (a of this section may contain optional adjuvant substances required in the production of such basic copolymers. These optional adjuvant substances may include substances permitted for such use by regulations in parts 170 through 179 of this chapter, substances generally recognized as safe in food, and substances used in accordance with a prior sanction or approval.

  (c Specifications. ? The methyl acrylate content is determined by an infrared spectrophotometric method titled Determination of Copolymer Ratio in Vinylidene Chloride/Methyl Acrylate Copolymers, which is incorporated by reference. Copies are available from the Center for Food Safety and Applied Nutrition (HFS-200? Food and Drug Administration, 5100 Paint Branch Pkwy., College Park, MD 20740, or available for inspection at the National Archives and Records Administration (NARA? For information on the availability of this material at NARA, call 202-741-6030, or go to:http://www.archives.gov/federal_register/code_of_federal_regulations/ibr_locations.html.

  ? The weight average molecular weight of the copolymer is not less than 50,000 when determined by gel permeation chromatography using tetrahydrofuran as the solvent. The gel permeation chromatograph is calibrated with polystyrene standards. The basic gel permeation chromatographic method is described in ANSI/ASTM D3536-76, Standard Test Method for Molecular Weight Averages and Molecular Weight Distribution of Polystyrene by Liquid Exclusion Chromatography (Gel Permeation Chromatography-GPC? which is incorporated by reference. Copies are available from University Microfilms International, 300 North Zeeb Rd., Ann Arbor, MI 48106, or available for inspection at the National Archives and Records Administration (NARA? For information on the availability of this material at NARA, call 202-741-6030, or go to:http://www.archives.gov/federal_register/code_of_federal_regulations/ibr_locations.html.

  ? Residual vinylidene chloride and residual methyl acrylate in the copolymer in the form in which it will contact food (unsupported film, barrier layer, or as a copolymer for blending will not exceed 10 parts per million and 5 parts per million, respectively, as determined by either a gas chromatographic method titled Determination of Residual Vinylidene Chloride and Methyl Acrylate in Vinylidene Chloride/Methyl Acrylate Copolymer Resins and Films, or, alternatively, Residual Methyl Acrylate and Vinylidene Chloride Monomers in Saran MA/VDC Resins and Pellets by Headspace Gas Chromatography, dated March 3, 1986, which are incorporated by reference in accordance with 5 U.S.C. 552(a? Copies are available from the Center for Food Safety and Applied Nutrition (HFS-200? Food and Drug Administration, 5100 Paint Branch Pkwy., College Park, MD 20740, or available for inspection at the National Archives and Records Administration (NARA? For information on the availability of this material at NARA, call 202-741-6030, or go to:http://www.archives.gov/federal_register/code_of_federal_regulations/ibr_locations.html.

  (d Extractives limitations. The basic copolymer resin in the form of granules that will pass through a U.S. Standard Sieve No. 45 ?50 microns shall meet the following extractives limitations:

  ? 10-gram samples of the resin, when extracted separately with 100 milliliters of distilled water at 121 C ?50 F for 2 hours, and 100 milliliters of n -heptane at 66 C ?50 F for 2 hours, shall yield total nonvolatile extractives not to exceed 0.5 percent by weight of the resin.

  ? The basic copolymer in the form of film when extracted separately with distilled water at 121 C ?50 F for 2 hours shall yield total nonvolatile extractives not to exceed 0.047 milligram per square centimeter ?.3 milligram per square inch?

  (e Conditions of use. The copolymers may be safely used as articles or components of articles intended for use in producing, manufacturing, processing, preparing, treating, packaging, transporting, or holding food, including processing of packaged food at temperatures not to exceed 135 C -?75 F?

  (f Other specifications and limitations. The vinylidene chloride-methyl acrylate copolymers identified in and complying with this section, when used as components of the food contact surface of any article that is subject to a regulation in parts 174 through 178 and 179.45 of this chapter, shall comply with any specifications and limitations prescribed by such regulation for the article in the finished form in which it is to contact food.

    [48 FR 38605, Aug. 25, 1983; 48 FR 50077, Oct. 31, 1983, as amended at 53 FR 47185, Nov. 22, 1988; 54 FR 24898, June 12, 1989]

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