当前位置: 首页? 政策法规? 国外法规? §177.1640 聚苯乙烯和用橡胶改性的聚苯乙烯(Polystyrene and rubber-modified polystyrene.)

§177.1640 聚苯乙烯和用橡胶改性的聚苯乙烯(Polystyrene and rubber-modified polystyrene.)

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放大字体缩小字体2011-10-11 04:10:00 来源9a href="http://www.law.cornell.edu/cfr/text/21/177/1640" target="_blank" rel="nofollow">GPO浏览次数9span id="hits">2781
核心提示:本节规定的聚苯乙烯和用橡胶改性的聚苯乙烯是基本聚合物。聚苯乙烯由聚苯乙烯聚合而成的基本聚合物组成。用橡胶改性的聚苯乙烯,由苯乙?丁二烯共聚物?或聚丁二烯与聚苯乙烯,无论在聚苯乙烯聚合过程中或聚合以后,共同结合而成的基本聚合物组成。可选辅料必须是170?89本部分中规定允许使用的物质、在食品中公认为安全的物质以及在法规、规定文件中允许使用的物质。本节还规定了聚苯乙烯和用橡胶改性的聚苯乙烯的质量指标、/div>
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备注 本节规定的聚苯乙烯和用橡胶改性的聚苯乙烯是基本聚合物。聚苯乙烯由聚苯乙烯聚合而成的基本聚合物组成。用橡胶改性的聚苯乙烯,由苯乙?丁二烯共聚物?或聚丁二烯与聚苯乙烯,无论在聚苯乙烯聚合过程中或聚合以后,共同结合而成的基本聚合物组成。可选辅料必须是170?89本部分中规定允许使用的物质、在食品中公认为安全的物质以及在法规、规定文件中允许使用的物质。本节还规定了聚苯乙烯和用橡胶改性的聚苯乙烯的质量指标、/td>

  177.1640 Polystyrene and rubber-modified polystyrene.


   Polystyrene and rubber-modified polystyrene identified in this section may be safely used as components of articles intended for use in contact with food, subject to the provisions of this section.

  (a Identity. For the purposes of this section, polystyrene and rubber-modified polystyrene are basic polymers manufactured as described in this paragraph so as to meet the specifications prescribed in paragraph (c of this section when tested by the method described in paragraph (d of this section.

  ? Polystyrene consists of basic polymers produced by the polymerization of styrene.

  ? Rubber-modified polystyrene consists of basic polymers produced by combining styrene-butadiene copolymers and/or polybutadiene with polystyrene, either during or after polymerization of the polystyrene, such that the finished basic polymers contain not less than 75 weight percent of total polymer units derived from styrene monomer.

  (b Optional adjuvants. The basic polymers identified in paragraph (a of this section may contain optional adjuvant substances required in the production of such basic polymers. Such optional adjuvant substances may include substances permitted for such use by regulations in parts 170 through 189 of this chapter, substances generally recognized as safe in food, and substances used in accordance with a prior sanction or approval.

  (c Specifications. ? Polystyrene basic polymers identified in paragraph (a)(1 of this section shall contain not more than 1 weight percent of total residual styrene monomer, as determined by the method described in paragraph (d of this section, except that when used in contact with fatty foods of Types III, IV-A, V, VII-A, and IX described in table 1 of 176.170(c of this chapter, such polystyrene basic polymers shall contain not more than 0.5 weight percent of total residual styrene monomer.

  ? Rubber-modified polystyrene basic polymers identified in paragraph (a)(2 of this section shall contain not more than 0.5 weight percent of total residual styrene monomer, as determined by the method described in paragraph (d of this section.

  (d Analytical method for determination of total residual styrene monomer content ? Scope. This method is suitable for the determination of residual styrene monomer in all types of styrene polymers.

  ? Principle. The sample is dissolved in methylene chloride. An aliquot of the solution is injected into a gas chromatograph. The amount of styrene monomer present is determined from the area of the resulting peak.

  ? Apparatus (i Gas chromatograph. Beckman GC-2A gas chromatograph with hydrogen flame detector or apparatus of equivalent sensitivity.

  (ii Chromatograph column. One-quarter inch outside diameter stainless steel tubing ?.028 inch wall thickness? 4 feet in length, packed with 20 percent polyethylene glycol ?0,000 molecular weight on alkaline treated 60-80 mesh firebrick.

  (iii Recorder. Millivolt range of 0-1, chart speed of 30 inches per hour.

  ? Reagents. Compressed air, purified; helium gas; hydrogen gas; methylene chloride, redistilled; and styrene monomer, redistilled.

  ? Operating conditions for the gas chromatograph. (i The column is operated at a temperature of 100 C with a helium flow rate of 82 milliliters per minute.

  (ii The hydrogen burner is operated with 15 pounds per square inch of air pressure and 7 pounds per square inch of hydrogen pressure.

  (iii The attenuation of the hydrogen flame detector is set at 210 2.

  ? Standardization. (i Prepare a standard solution by weighing accurately 15 to 20 milligrams of styrene monomer into a 2-ounce bottle containing 25.0 milliliters of methylene chloride. Cap the bottle tightly and shake to thoroughly mix the solution.

  (ii By means of a microliter syringe, inject 1 microliter of the standard solution into the gas chromatograph. Measure the area of the styrene monomer peak which emerges after approximately 12 minutes.

  ? Procedure. (i Transfer 1 gram of sample (accurately weighed to the nearest 0.001 gram to a 2-ounce bottle and add several glass beads. Pipette 25.0 milliliters of methylene chloride into the bottle. Cap the bottle tightly and place on a mechanical shaker. Shake until the polymer is completely dissolved. If any insoluble residue remains, allow the bottle to stand (or centrifuge at a low speed until a clear supernatant layer appears.

  (ii By means of a microliter syringe, inject 3 microliters of the clear supernatant liquid into the gas chromatograph.

  (iii Measure the area of the resulting styrene monomer peak. Compare the sample peak area with the area produced by the standard styrene monomer solution. Calculation:

  Percent residual styrene monomer=Milligrams monomer in standardpeak area of sample/Peak area of monomer standardsample weight in grams30

  (e Other specifications and limitations. The polystyrene and rubber-modified polystyrene identified in and complying with this section, when used as components of the food-contact surface of any article that is the subject of a regulation in parts 174, 175, 176, 177, 178 and 179.45 of this chapter, shall comply with any specifications and limitations prescribed by such regulation for the article in the finished form in which it is to contact food.

  (f Nonapplicability. The provisions of this section are not applicable to polystyrene and rubber-modified polystyrene used in food-packaging adhesives complying with 175.105 of this chapter.

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