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U_(uSvؚ0xn[mkGSpe0V 1 mol/L ؚ0xn[m1 mlvS_N0.3350 gIx (u N_{vQSm^  EMBED Equation.3  _-NC:Nؚ0xn[mSm^ mol/L m:NIx(ϑ gV:Nؚ0xn[mSOy ml0 2.2.1.3.4 kxx (H2SO4) n[m (1) M6R0.25 mol/Lkxxn[me Skxx15 ml lv g4lvpogXleQ4l-N0_nm)n^M[)n QR4lzʑ1000 ml GdS0 (2) h[Sm^e yS~270!^300!pr^R`͑vWQe4lxx0.8 g(|nx0.0001 g) n250 mlxϑt-N R4l50 ml On0R2uW~-n2uZ~mTc:ym1 g/L 2uW~YNnm20 mlN2g/Ln2uZ~YNnm30 mlmS 10 n (uM6Rvkxxn[mňeQ50 mln[{-N n[0_nm1u~rlS:N+}~re nql2 min0QtS[)nT ~~n[nm1u~rS:Nf+}r U_(uSvkxxn[m;`kGSpe0V1 mol/Lkxxn[m1 mlvS_N0.1060 g e4lxx c N_{kxxn[mSm^  EMBED Equation.3  _-NC:Nkxxn[mSm^ mol/Lm:Ne4lxx(ϑ gV:Nkxxn[mSOy ml0 2.2.1.3.5 "l'lS (NaOH) n[m (1) yS37 g "l'lS R4l/cGd Onb50 mlqTnm0QtST nZYNpQXet-N Ynpee_on0M6R0.1 mol/L"l'lSn[me Sonv"l'lSqTnm5.6 ml R4lb1000 ml GdS0 (2) h[Sm^e yS~105!pr^R`͑vWQN2ux"l0.4 g (|nx 0.0001 g) n250 ml xϑt-N0R4l50 mln R2nZ^c:ym(1 g Z^ RYNnb100 mlnm) (u"l'lSn[m(ňN50 mlx_n[{-N)n[0_nmHT~re U_(uSv"l'lSn[mkGSpe0V1 mol/L"l'lSn[m1 mlvS_N0.2042 g N2ux"l c N_{vQSm^  EMBED Equation.3  _-NC:N"l'lSn[mSm^ mol/Lm:NN2ux"l(ϑ g V:N"l'lSn[mSOy ml0 2.2.1.3.6 ؚ/lx (HCLO4) n[m (1) M6R0.1 mol/Lؚ/lxn[me SQx750 ml ReQؚ/lx(Sm^:N70%^72% ) 8.5 ml /cGdOmS0(W[)n NnRP(RGd)23 mlT GdS0_QtST RQxOb1000 mlnm GdS >en24 hTh[vQSm^0 (2) h[Sm^e yS~105!pr^R`͑vWQN2ux"l0.4 g(|nx 0.0001 g) n100 mlxϑt-N RQx20 mlOn R~vf+}c:ym(0.5 g~vf+}(uQxnb100 mlnm)1n (uM6Rvؚ/lxn[m(ňN25 mln[{-N)n[0_nm1u+}rSb݄re U_(uSvؚ/lxn[mkGSpe0 Te O(u N+TN2ux"lvQx͑ Y Nd\O(zz}v[gq)0V1mol/Lؚ/lxn[m1 mlvS_N 0.2042 g N2ux"l (u N_{vQSm^  EMBED Equation.3  _-NC:Nؚ/lxn[mSm^ mol/Lm:NN2ux"l(ϑ gV10V2:N7h,g~Nzz}v~(uSؚ/lxn[mSOy ml0 2.2.1.3.7 V|x [(C6H5)4BNa] n[m (1) M6R0.02 mol/L V|xn[me ySV|x7.0 g R4l50 ml /cGdOn0ReQeM6Rv"l'lSݔQ(S N/lSݔ1.0 g nN25 ml 4l-N0(W Nedb NnR"l'lSՋmpH:N 8^9 N/lS16.6 g EQRdbGWS06qT R4l250 ml /cGd15 min0Yn10 min Ǐn0Snm v^nR"l'lSՋmpH :N8^9 QR4lzʑ1000 ml GdS0 (2) h[Sm^e |nxϑS,gm10.0 ml Rx-xQm(Se4lx 20g R4l300 mln0RnZ݄c:ym1 mlNQx60 ml^80 ml nmN݄rS:N~~r QR4lzʑ1000 ml pH 3.7) 10 mlNnZ݄c:ym0.5 ml0(u0.01 mol/Lpvn[m(2.2.1.3.8) n[݄r0 TeZP N+T,gmvzz}vՋn[0V1 mol/LV|xn[m1 mlvS_N1 mol/Lpvn[m1 ml EeS c N_{vQSm^  EMBED Equation.3  _-NC:NV|xn[mSm^ mol/LV10V27h,g~Nzz}v~(uSpvSOy mlC1:Npvn[mSm^ mol/LV:NϑSV|xn[mvSOy ml0 2.2.1.3.8 pv (C22H40ClN) n[m (1) M6R0.01 mol/Lpvn[me S/lSN2uWĂWp3.8 g R4lOn0QRx-xQm(pH 3.7)10 ml v^R4lzʑb1000 ml GdS0 (2) h[Sm^e yS~150!pr^1 hvRg~/lS0.18g(|nx0.0001 g) n250 ml [ϑt-N Rx-xQm(pH 3.7) Onv^zʑ;R^ GdS0|nx8TSzʑm20.0 ml n50 ml [ϑt-N |nxR0.02 mol/L V|xnm25.0 ml QR4l;R^ GdST~r^qn~Ǐn0_SRnm |nxS~nm25.0 ml n 250 ml xϑt-N RnZ݄c:ym0.5 ml (uM6Rvpvn[mn[0_nmHT݄re U_(uSvpvn[mkGSpe0 Te (u N+T/lSvx-xQm͑ Y Nd\O(zz}v[gq)0V1 mol/Lpvn[m1 mlvS_N0.07455 g /lS EeS(u N_{pvn[mSm^  EMBED Equation.3  _-NC:Npvn[mSm^ mol/Lm/lS(ϑ gV10V2:N7h,g~Nzz}v~(uSpvn[mSOy ml0 2.2.1.3.9 xxKIO3 n[m M6R0.05 mol/Lxxn[me \WQxx(W105!r^qR`͑T |[yS10.700 g n1000 ml [ϑt-N0Rϑ4lOn Qzʑ;R^ GdS sS_0 2.2.1.4 pH75%)R`)n{Q3*Ng b 54!R`)n{Q14d0N>enMR0TR+RKm[mkBR@g̃ gHebR+Tϑ0k!khKm7hT:N Nyb kyb7hT͑ YKm2!k SvQs^GWe3*Ngv7h,g vQ@g̃ gHebR+Tϑ NMsd"10% S\.X[ gHeg[:N2t^~54!X[>e14d @g̃ gHebR NMsd"10% R.X[ gHegS[:N1t^0 (3) *gǏ,gՋvmkBR b2k‰[2t^N NPX[ gHegvmkBR S c N[)nYu7hl2.2.3.2.2 Km[vQPX[ gHeg0 (4) Km[~g^[vQ'`rSSۏLc V grI{'`rSS elۏL gHebR~lKm[e N[)nYu7hl~g:NQ0 2.2.3.2.2 [)nYu7hl S]Km gHebR+Tϑv^Sň}YvmkBR >en)n^:N25!2!sX (U_)n^) cNTOX[gePONcO S7hKm[ gHebR+Tϑ gHebR+Tϑ NMsd"10%:NǏ0 2.2.3.3 _uirKm[l (1) .X[elTS7hBl TSf[Km[l(2.2.3.2)0 (2) (W@gmpbb6R_uirՋ-N @b(uՋ_uir^:NO(uffN-Nb@gmpbb6R_uir-NbRg:_0 (3) [SO(uSmmkvmkBR vc(uvQSmۏL@g̃bb̃Ջ0[zʑTO(uvmkBR RNvQO(uffN-N@g̃Ten3Gr7hGr0xmle Tyё^\kN7hGrv1 cmN N S(W TN[hVQ(+T600 mlmkm) ۏL0 (5) xml0Rĉ[eT SQё^\Gr HQ(ueg4lQm Q(uk7RbvQ[o'`hVwQSdPNir0YN gnd NcvPNir S cGB 10124-88@bN~v NRelnd: ܔGr: (W[)n NxmlNvxnm(500ml 36%^38% vxR4l1000ml vxk͑:N1.19)-N1min^3min0 xGrn+T |200 g/Lv"l'lSnm-N nql5 min^30 min0 ݔGrxmlN N'lSxxnm( N'lS20 g xx500ml R4l1000ml0xxk͑:N1.69)-N GS)n80! 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4)eh^^mmSFmTQO(uS YO(uvSňPgeT[hV ^~nmTMbSQ!kO(u 5)v0v0xI{hVv{|irT =\ϑUS*NSňSňe^\vSb__{Y*NSň(WNwe @b(uhVvv_S^gTN*NeT^d>ee hVv(u8Tnk]b~^_ N)R}lneQ 6)mp̃irTbxSv_{bxS Y[l\hVۏLSňe {^bQ0_{f2irTvT*NhbYjRRT@{_{EQRd_ N)Rmp̃VP[c@b girSOhb0 g[{T[v[hV ^\vSb_ _ST NbO>e0{T{|irTY[{0T{TQHQ(u4lbSyP[4lmn 6qTzsSmp̃ 7)irTFcNb N[Ǐ'} Y(uSf[c:y&^4\ mp̃Sk'YSQTmkMOvSQ>enSf[c:yir0 (3)ň} 1) Nclmp̃hVvň}ϑ N_Ǐg[Q[ϑv80% wzzmp̃hVvň}ϑ N_Ǐg[[y90% TewzzT RwzzSR}lmp̃hVvň}ϑSR+R N_\Ng[[yv10%T5% N2bk \ňϑHe^ kYuzzlq_Tmp̃Heg 2)^=\ϑ\ T{|irT>e(WNwmp̃ _{\ N T{|irTň>e(WNw RNg0Rmp̃irT@bv)n^Te:NQ 3)irTň>ee N N]SvNGW^N[ݍyN)R}lnbczzl'YWmp̃hV irT^>eNg[bcf Nv}irg Ne}irgv-N\Wmp̃hV S\irT>eNQ{-N 4)Nmp̃v'YS>e(W NB\ fmp̃v\S>e(W NB\ё^\irT>e NB\ ~irS>e NB\ irTň>e N4`蕌TVX N28TeQYvQQ4l 5)ё^\S^s^>e v0x0xI{^YNzzvMOn~~~ir^ObSveTN4ls^bbWvr`sttI{^_ST NbO>eN)R}lۏeQTzzlcQ 6)/T_[{T[[hV ^\[{T[vvSb_0 (4)mp̃Yt 1)}lv(ϑBl0_{[ňl4lRyhV mp̃Ǐ z-N}lvqT^Tf4l nvS N\O:NẽSO(u/T_[hV hg[{T[/f&T]sQ b$hgSf[c:y&^Sr`Q *g0Rb gSup NS\O:NẽSS>ey[O(u_SO(uMR^hgSQc:yaS/f&T0R]mp̃vrlbr` *g0Rb gup NS\O:NẽSO(u c$mp̃Sc=(W0W b>e NmKNYbl g4lm GW^Ɖ:NS0Ralg NS\O:NẽSO(u d$]mp̃virT N_N*gmp̃irTm>e e$Te v^R2\i N2Qalg h$mp̃TvirT ^>eeQmQ:Svgqj(bgP[ N cfQ)gqjbgP[^1u Nf8Tno0hbIQmvPge6Rb hbQmN NfeR1=vme OKNfNnmTmkmp̃irT^>eNy0Wؚ20cm^25cm y)Yg50cm yX܏N5cmYv}irg N z^c>e R{|>en v^Rv2\iẽirTPX[(W[gSv^ gnmNmkce N[N(u NN# P6ResQNXTQeQ i$PX[v gHegSSňPge0\Sv%N['`0mp̃agN0PX[sXI{YV }q_Th^SňPgeT_/T_[hV N,^ )n^25!N N10d^14d nonYc[^)w)YpevQ[SňPgeYN!k'`e~^N!k'`~QXSňPge Y[SňPge;!c_uirneQ vQ gHegSv^^ \:NJSt^N N0 3.1.2 r^pmp̃ 3.1.2.1(uV(uNؚ)n N N_cOW0 NS(0 NSirTvmp̃(uN NnpvhVhvmp̃(uN}lblSO NzirTvmp̃ Yst0l0|BRTё^\I{6RTvmkmp̃0 3.1.2.2 mp̃el 1 p|p(uNؚ)nirT0\Nё^\hVhvmp̃0 2 r^p(ur^pmp̃{ۏLmp̃ mp̃agN:N160! 2h b170! 1hb180! 30min0YǑ(u:gh[AmWp{0 3 laNy_mp̃virTr^pmp̃MR^mQ 2bk bmp̃1Y%balirpSsthVvmp̃MR^mQv^r^qmp̃eRNp{^SVXc mp̃T_)n^M0R40!N NQ_{ N2bkpˆ0 irTSň NǏ'Y NǏ10cm10cm20cm irT NǏp{vؚ^v2/3 irT^Yu gEQRvzzS>eeQNSKb lBR0|BRvS^ N_Ǐ0.635cmQXg~^agS^ N_Ǐ1.3cm0 )n^ؚN170!e g:girOxS0Ee g:girTmp̃e )n^ NSǏؚ0 3.1.3 Sal Sal1\/fǏirtTSf[el\mirT N g:gir0e:girT_uir=\S0WMNO0Rk[hQv4ls^0nm{_^/fOmkbmp̃bRvsQ.0 3.1.3.1 q_TV } 1 irT,gv YBg'` Y{TThb NIQnvirT_nmN,`Q N YBgirT_{=\Sb N (u+TvmmBRxmlTKb]N~7Rm0 2 alg_uirvpeϑT{|W0 3 irT NkYu g:girvpeϑTrQ g:girOq_Tmp̃vbR g:girY Rmp̃bRvS'`\YirT N g:girSr^ Rnme_\ g:gir{_^Sd0 3.1.3.2Salvel (1)eg4lnmSOc@I{algirnon FO[oSbSdr^valireHeeg4lS(uNalg{0e g:giralg0hbIQnirTvnm0 (2)nmBRSOc@I{algirnon ~gr^valir FOMTvQ[:gh;mRSdalir0la_YnmBR$\vQ/f[(ummBR gN[P'` O(ue^2bk[ё^\hVh$\vQ/fNN|[;SuNhVv4xOW0 (3)vnmBRvS gHe0WR㉌TSdr^Tnmvalirv gUSvTYv MRSRalir-Nvˆ}v( TSR@b gv g:galir0YMTO(uꁨRnmhV0XlI{ RnmHegfsO0v;N(uNalg͑0$\vQ/f g:giralg0irT~g YBghb NIQnirTvnm0 (4) pH < 7vmmBR;N(uNe:galirvnmpH > 7vmmBR;N(uN g:galirY@0T|Ovnmё^\hVh;N b1_x'`mmBR0 3.1.3.3 SalvǏ zSb6*NekR{|0xml0nm0(ueg4lom0(uSyP[4lom0r^q (1)R{|g}YO(u[ksSۏLR{| =\ϑ Nvc(uKbۏLR{|)RirT_{>e(W2:R[hVQۏLЏalirOcnm2bkr^q Y N(W1h^2hKNQSenm {\irTxmNQ4lb+TvmSO-N0 (2)xmlxmlS2bkalirSr^ToSbSdalir g'Yϑ 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